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All rights reserved. Super Flangeless? Thermo Fisher Scientific Inc. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

The contents of this document are subject to change without notice. All technical information in this document is for reference purposes only.

System configurations and specifications in this document supersede all previous information received by the purchaser. This document is not part of any sales contract between Thermo Fisher Scientific Inc. This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of Sale shall govern all conflicting information between the two documents.

Release history: First release April Software versions: Xcalibur 2. Not regulated for medical or veterinary diagnostic use by U. Federal Drug Administration or other competent authorities. Regulatory Compliance Thermo Fisher Scientific performs complete testing and evaluation of its products to ensure full compliance with applicable domestic and international regulations.

When the system is delivered to you, it meets all pertinent electromagnetic compatibility EMC and safety standards as described below. Changes that you make to your system may void compliance with one or more of these EMC and safety standards.

Changes to your system include replacing a part or adding components, options, or peripherals not specifically authorized and qualified by Thermo Fisher Scientific. To ensure continued compliance with EMC and safety standards, replacement parts and additional components, options, and peripherals must be ordered from Thermo Fisher Scientific or one of its authorized representatives.

CAUTION Read and understand the various precautionary notes, signs, and symbols contained inside this manual pertaining to the safe use and operation of this product before using the device. Notice on the Susceptibility to Electromagnetic Transmissions Your instrument is designed to work in a controlled electromagnetic environment. Do not use radio frequency transmitters, such as mobile phones, in close proximity to the instrument.

It is marked with the following symbol: Thermo Fisher Scientific has contracted with one or more recycling or disposal companies in each European Union EU Member State, and these companies should dispose of or recycle this product. See www. WEEE Konformit? C Contents Preface. Fleet system. This manual provides information on how to connect your LCQ Fleet system. To access the Help, choose Help from the menu bar or click the button on the toolbar.

Safety and Special Notices Make sure you follow the precautionary statements presented in this guide. The safety and other special notices appear in boxes. Note Highlights information of general interest. Tip Helpful information that can make a task easier.

Contacting Us There are several ways to contact Thermo Scientific. Assistance For new product updates, technical support, and ordering information, contact us in one of the following ways: Visit Thermo Scientific on the Web www. Contact Customer Service For ordering information in the U. Fill out a reader survey online at www. Send an e-mail message to the Technical Publications Editor at techpubs. This chapter contains the following sections:?

Connecting the Forepump? Connecting the Gases to the MS Detector? Turn the Main Power circuit breaker to the Off O position. See Figure 3 on page 5. Make sure that the Electronics switch is in the Service Mode position. Connect the male plug of the power cord to the V ac power source in your laboratory. CAUTION If your local area is subject to power fluctuations or power interruptions, you must install a power conditioning device or an uninterruptible power supply UPS in your laboratory.

Connecting the Vacuum Hose? Connecting the Forepump to the Laboratory Exhaust System? Table 1 lists the components and Figure 1 shows the components of the vacuum hose assembly. The adapters at the two ends of the vacuum hose assembly are connected at the factory. Table 1. ID, 8 ft. OD for the end that is inserted into the vacuum hose, 1. OD for the end that is inserted into the vacuum hose, 2.

To connect the vacuum hose to the MS detector a. Place the 41 mm 1. To connect the other end of the vacuum hose to the forepump a. Place the 26 mm 1. Figure 2 shows the connection between the vacuum port of the MS detector and the exhaust port of the forepump. Most atmospheric pressure ionization API applications contribute to the accumulation of solvents in the forepump.

While it is recommended that you periodically open the ballast valves on the top of the pumps to purge the accumulated solvents, opening the valves might allow a large volume of volatile solvent waste to enter the fume exhaust system.

Choose an exhaust system that can accommodate the periodic purging of these solvents. The frequency of the purging depends on the throughput of your system. To connect the exhaust port of the forepump to the laboratory exhaust system 1.

ID blue exhaust hose to the forepump exhaust port. Vent the free end of the blue exhaust hose to an external exhaust system in your laboratory. The exhaust hose should travel at floor level for a minimum of two meters This tubing acts as a trap for exhaust fumes that would otherwise recondense in the forepump oil.

Figure 2 shows the blue exhaust hose connected to the optional oil mist filter, which is connected to the exhaust port of the forepump. Figure 2.

The power outlet for the forepump is located on the power entry module of the MS detector. To connect the forepump to line power the forepump outlet of the MS detector : 1. On the power entry module, switch the Main Power circuit breaker to the Off O position.

Connect the power cord plug of the forepump to the Mechanical Pump power receptacle of the MS detector. Turn on the power switch of the forepump. Figure 3. Pumps A 5. Figure 4. Connecting the Nitrogen Source? Because nitrogen gas usage can be quite high, Thermo Scientific recommends one of three nitrogen sources: a large, sealed, thermally insulated cylinder containing liquid nitrogen from which the nitrogen gas is boiled off; the largest nitrogen cylinder that can be practically used; or a nitrogen generator.

ID Teflon? See Figure 5 for the proper orientation of the fitting and ferrule. To connect the tubing, align the Teflon tubing with the opening in the fitting and firmly push the tubing into the fitting until the tubing is secure. Because particulate filters can be a source of contamination, Thermo Scientific does not recommend their use. You can dispense helium from a tank containing ft3 of gas, using a Matheson Series1 regulator or equivalent tank and regulator.

Whether you choose copper or stainless steel gas lines for the helium, use gas lines that are free of oil and preferably flame dried. Connect the opposite end of the tubing to the helium gas source, using an appropriate fitting.

Figure 5. To connect the MS detector to the data system computer 1. Connect the Ethernet switch to line power. Connect the 1-in.

ID Tygon? Insert the other end of the tubing into a waste container, and vent the waste container to a fume exhaust system. Always ensure that the PVC drain tubing is above the level of liquid in the waste container. Do not vent the PVC drain tube connected to the waste container to the same fume exhaust system to which you have connected the forepump.

Connecting the API source drain tube and the forepump exhaust to the same fume exhaust system is likely to contaminate the analyzer optics. Equip your laboratory with at least two independent fume exhaust systems. Route the blue exhaust tubing from the forepump to a dedicated fume exhaust system. Vent the waste container to a dedicated fume exhaust system that is independent from that used for exhausting the forepump.

External devices include devices controlled or not controlled from the Xcalibur data system. Table 2 lists the Xcalibur kits for various external devices.


LCQ Fleet Ion Trap Mass Spectrometer Support

Thermo Fisher Scientific Inc. Chromatography Thought spiders were mere creepy crawlies? This reliable and easy-to-use ion trap mass spectrometer, from the inventors of the technology, provides maximum information in minimum time with exceptionally low levels of sample consumption. Furthermore, the Ion Max tm source delivers outstanding robustness for the most demanding analytical applications. What Are the Biggest Scientific Breakthroughs of?


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